Fractionating Column Packing
Learn more about our column packing options and Pope’s Pro-Pak distillation column packing.
Standard Distillation Column Packings
A range of packing types for fractional packed column systems is available. The standard distillation column packing offered is Pro-Pak® random packing. Customer-specified packings can be used including materials of stainless steel, metal alloys, ceramic, and plastics.
Typical Column Packing Equipment Options
- Pro-Pak® distillation column packing
- Saddles
- Rings
- Structured Packing
- Knitted Packing
Non-Random Packings Available Include:
- Woven wire mesh, spiral rolled type cylindrical sections.
- “Structured” corrugated sheet or gauze metal cylindrical sections.
- Bubble-cap or sieve tray plates.
As a generality, smaller diameter columns favor small-size random packings such as Pro-Pak® for higher efficiency, as opposed to large-size random or non-random types due to column wall effects.
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Properties, Performance and Specifications of 0.24″ Protruded Pro-Pak® Standard Packing
- Material of construction, 316 stainless steel (monel, other alloys available).
- 372 ft2 per 1 ft3 of packing, allowing high mass transfer rates.
- 96% free space, allowing low pressure drop, especially in vacuum distillation.
- Shape: half-cylinder, corners bent.
- Size: 0.24″ diameter x 0.24″ length, 0.003″ sheet thickness, 1,024 protrusion holes per in2.
- Density: 290,000 pieces and 21 lb/ft3, (316 SS).
- Packing factor: 420.
- Flood rate predicated with the following equation:
- G=270(ρ1)0.58(ρg)0.42where:
- G=Mass vapor velocity, lb / ft2 • hr
- ρ1=Density of liquid phase, lb/ft3
- ρg=Density of gas phase, lb/ft3
- Efficiency of the packing increases with increasing vacuum.
Comparative Column Packing using PRO-PAK®
Column Diameter (inches) | Operating Pressure | Boil Up Rate(L/hr) | Vapor Velocity(ft/sec) | HETP (Plate Height Inches) | Pressure Drop (Inches H20/ft) |
---|
2 | atmospheric | 3.7 | 0.35 | 1.77 | 0.12 |
2 | atmospheric | 15.5 | 1.46 | 2.10 | 1.70 |
2 | (200 mm Hg) | 1.05 | 0.31 | 0.79 | 0.23 |
2 | (200 mm Hg) | 11.15 | 3.20 | 1.33 | 5.23 |
2 | (50 mm Hg) | 4.6 | 4.70 | 0.92 | 2.54 |
6 | atmospheric | 37.0 | 0.40 | 1.66 | 0.18 |
6 | atmospheric | 146.0 | 1.60 | 2.57 | 2.86 |
* Above data obtained at Total Reflux with 0.24″ PRO-PAK®
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Fractional Distillation Gallery
View our gallery of Fractional Distillation systems including batch and continuous mode systems.
Turnkey skid for distillation of biomedical polymers used in implantable devices. All 316L SS except for dual glass receivers.
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